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CWEA GRADE 1 LAB ANALYST PRACTICE TEST 4 QUESTIONS WITH CORRECT ANSWERS, Exams of Water Resources Planning and Management

CWEA GRADE 1 LAB ANALYST PRACTICE TEST 4 QUESTIONS WITH CORRECT ANSWERS

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CWEA GRADE 1 LAB ANALYST PRACTICE TEST 4
QUESTIONS WITH CORRECT ANSWERS
1) Which of the following best describes the interpretation for total coliform and E coli
for the enzyme-substrate test? -- Answer โœ”โœ” The presence of fluorescence is a
positive test for E. coli. If the chromogen intensifies, the sample is total-coliform
positive.
2) What is a Grab sample? -- Answer โœ”โœ” Single samples collected at a specific spot at a
site over a short period of time (not to exceed 15 min)
3) A sample is in a person's custody if it is: -- Answer โœ”โœ” In the individual's physical
possession, sight, secured and tampered proof by that individual, or secured in an
area restricted to authorized personnel
4) What should sample labels include? -- Answer โœ”โœ” Unique sample number, sample
type, name of the collector, date and time of collection, place of collection, and
sample preservative
5) Sample seals should include -- Answer โœ”โœ” Sample number that is identical to sample
label, collector's name, date and time of sampling. Attach so it must be broken to
open sample container.
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CWEA GRADE 1 LAB ANALYST PRACTICE TEST 4

QUESTIONS WITH CORRECT ANSWERS

  1. Which of the following best describes the interpretation for total coliform and E coli for the enzyme-substrate test? -- Answer โœ”โœ” The presence of fluorescence is a positive test for E. coli. If the chromogen intensifies, the sample is total-coliform positive.
  2. What is a Grab sample? -- Answer โœ”โœ” Single samples collected at a specific spot at a site over a short period of time (not to exceed 15 min)
  3. A sample is in a person's custody if it is: -- Answer โœ”โœ” In the individual's physical possession, sight, secured and tampered proof by that individual, or secured in an area restricted to authorized personnel
  4. What should sample labels include? -- Answer โœ”โœ” Unique sample number, sample type, name of the collector, date and time of collection, place of collection, and sample preservative
  5. Sample seals should include -- Answer โœ”โœ” Sample number that is identical to sample label, collector's name, date and time of sampling. Attach so it must be broken to open sample container.
  1. Field log books should include: -- Answer โœ”โœ” Purpose of sampling, location of sampling point, name and address of field contact, producer of material being sampled and address, type of sample, method, date, and time of preservation
  2. The chain of custody should include -- Answer โœ”โœ” Sample number, signature of collector, date, time, and address of collection, sample type; sample preservation requirements; signatures of person involved in the chain of possession, and inclusive dates and times of possession
  3. The laboratory portion of the sample analysis request sheet should include -- Answer โœ”โœ” Name of the person receiving the sample, laboratory sample number, date of sample receipt, condition of each sample, and determinations to be performed
  4. When should samples be delivered? -- Answer โœ”โœ” As soon as practicable after collection, typically within 2 days and have chain of custody record
  5. Procedure for receiving samples -- Answer โœ”โœ” Inspect condition, seal, and review label against chain of custody forms. Assign lab number and log into log book or LIMS. Store in secure storage room.
  6. What is the Sampling protocol for alkalinity? -- Answer โœ”โœ” Plastic, glass, fluoropolymer, cool to </= 6 C
  7. What is the Sampling protocol for BOD? -- Answer โœ”โœ” Plastic, glass, fluoropolymer, cool to </= 6 C
  8. What is the Sampling protocol for COD? -- Answer โœ”โœ” Plastic, glass, fluoropolymer, analyze ASAP, or add H2SO4 to pH <2, cool to </= 6 C
  1. pH sample prep for BOD -- Answer โœ”โœ” If not between 6.0 and 8.0 adjust sample temp to 20+/-3 C, then adjust pH to 7.0 to 7.2 using sulfuric acid (h2SO4) or sodium hydroxide (NaOH)
  2. Residual Chlorine in samples for BOD -- Answer โœ”โœ” Dechlorinate sample using Na2SO3 solution
  3. Samples with Hydrogen peroxide with DO -- Answer โœ”โœ” Mix samples vigorously in open containers for sufficient time to allow hydrogen peroxide levels to dissipate
  4. Seed suspension for BOD analysis -- Answer โœ”โœ” Preferred seeds include supernatant from settled domestic wastewater, effluent from primary clarifiers, diluted mixed liquor from an aeration basin, disinfected effluent, or receiving water from below the point of discharge
  5. Dilution water preparation for BOD -- Answer โœ”โœ” - DO concentration is 7.5 mg/L
  • Add 1 mL each of phosphate buffer, MgSO4, CaCl2, and FeCl3 solution/L to prepared source water
  1. Sample temperature adjustment for BOD -- Answer โœ”โœ” Bring samples to 20 +/-3 C
  2. Samples that require nitrification inhibition -- Answer โœ”โœ” Biologically treated effluents, samples seeded with biologically treated effluents, and river water
  3. Sealing BOD bottles -- Answer โœ”โœ” Fill each bottle enough to where insertion of stopper leaves no bubbles in bottle. Mix sample by turning bottle manually several times
  4. Initial DO measurement -- Answer โœ”โœ” Measure initial DO within 30 minutes after preparing dilution
  1. Incubation of BOD -- Answer โœ”โœ” Incubate at 20 +/- 1 C without light for 5 days +/- 6 hours
  2. Valid data of BOD analysis -- Answer โœ”โœ” - Minimum depletion of 2.0 mg/L DO
  • Residual DO of 1.0 mg/L
  1. The primary basis of precision and accuracy in BOD analysis -- Answer โœ”โœ” Glucose- glutamic acid check
  2. Definition of pH -- Answer โœ”โœ” The negative logarithm of the hydrogen ion concentration in moles per liter (pH=-log[H+])
  3. One unit change in pH represents what -- Answer โœ”โœ” A ten fold change in the concentration of the hydrogen ion
  4. Calibration of pH instrument -- Answer โœ”โœ” Use two buffers which bracket the expected pH value for greatest accuracy
  5. Temperature instruments -- Answer โœ”โœ” Mercury filled glass thermometers with scale markings at a minimum of every 0.1 C
  6. How is hardness measured? -- Answer โœ”โœ” Using EDTA titrimetric method. 1. pH of sample is buffered to 10 +/- 0.1 and Eriochrome black T is added as an indicator. Mohs hardness scale
  7. Endpoint of EDTA titrimetric method for hardness -- Answer โœ”โœ” Indicator turns red to purple, meaning all Ca and Mg have been chelated
  8. Units of hardness -- Answer โœ”โœ” mg/L CaCO
  1. Holding time for BOD -- Answer โœ”โœ” 48 hours
  2. Holding time for COD -- Answer โœ”โœ” 28 days
  3. Holding time for chloride -- Answer โœ”โœ” 28 days
  4. Holding time for chlorine, total, residual -- Answer โœ”โœ” 0.25 hours
  5. Holding time for color -- Answer โœ”โœ” 48 hours
  6. Holding time for odor -- Answer โœ”โœ” 24 hours
  7. Holding time for pH -- Answer โœ”โœ” 0.25 hours
  8. Holding time for solids -- Answer โœ”โœ” 7 days
  9. Holding time for temperature -- Answer โœ”โœ” 0.25 hours
  10. holding time for turbidity -- Answer โœ”โœ” 48 hours
  11. Interference of turbidity analysis -- Answer โœ”โœ” Dirty bottles
  12. pH meter ranges -- Answer โœ”โœ” Should be reproducible to 0.1 pH unit and range of 0 - 14
  13. Short-term storage of pH electrode -- Answer โœ”โœ” pH 4 buffer
  1. pH meter calibration -- Answer โœ”โœ” 1. Place in initial buffer solution and set isopotential point
  1. Select second buffer within 2 pH units